{"id":972,"date":"2014-10-30T09:42:08","date_gmt":"2014-10-30T07:42:08","guid":{"rendered":"http:\/\/blogs.sun.ac.za\/ctscanner\/?p=972"},"modified":"2017-10-18T14:19:44","modified_gmt":"2017-10-18T12:19:44","slug":"particle-size-distribution-analysis","status":"publish","type":"post","link":"https:\/\/blogs.sun.ac.za\/ctscanner\/particle-size-distribution-analysis\/","title":{"rendered":"Particle size distribution analysis"},"content":{"rendered":"<p>X-rays imaging at high resolution allows visualization and quantification of any type of sample, including particles and powders. X-ray computed tomography in the micro and even nano scale is now possible, as a service facility in Stellenbosch University. Here we present the advantages of using the method for particles and powder characterization.<\/p>\n<p>The full 3D data set is first analyzed in greyscale slice images. These images immediately show the user the general morphology of the grains of interest, also showing internal features such as porosity or dense inclusions within particles. The slice images are equivalent to \u201cthin sections\u201d through the middle of the scan field of view, and you can \u201cscroll through the object\u201d without any special software. In the sugar grains we see no internal porosity or density variations, but many flat surfaces on the particles. In the 3D image, the largest 3 sugar grains are selected from analysis and extracted to view them seperately in 3D.<\/p>\n<p><a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-slice.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-large wp-image-973\" src=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-slice-1024x741.jpg\" alt=\"sugar slice\" width=\"1024\" height=\"741\" srcset=\"https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-slice-1024x741.jpg 1024w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-slice-300x217.jpg 300w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-slice.jpg 1424w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/p>\n<p><a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-3D.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-large wp-image-974\" src=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-3D-1024x733.jpg\" alt=\"sugar 3D\" width=\"1024\" height=\"733\" srcset=\"https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-3D-1024x733.jpg 1024w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-3D-300x214.jpg 300w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/sugar-3D.jpg 1440w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/p>\n<p>The concrete powder shows very irregular shapes with pores inside some particles. A particle size distribution analysis is performed, and the histogram shown below. In addition to particle volume or diameter, every particle has its 3D surface area, X,Y,Z projection area, longest axis length, sphericity factor, etc. calculated. All this additional information can be very useful and is not possible with any other technique such as surface analysis \u201ctopography\u201d SEM or laser methods, all of these have some limitations in providing real shape information in true 3D. The only limitation to X-ray CT is the field of view and resolution. Best resolution is 500-1000 nm which is possible using a 1 mm sample size, and makes possible quantitative size distribution analysis of 10 \u2013 1000 micron particle diameters.<\/p>\n<p><a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-slice.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-large wp-image-975\" src=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-slice-1024x364.jpg\" alt=\"concrete powder slice\" width=\"1024\" height=\"364\" srcset=\"https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-slice-1024x364.jpg 1024w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-slice-300x106.jpg 300w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-slice.jpg 1418w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/p>\n<p><a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-analysis.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-large wp-image-976\" src=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-analysis-1024x364.jpg\" alt=\"concrete powder analysis\" width=\"1024\" height=\"364\" srcset=\"https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-analysis-1024x364.jpg 1024w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-analysis-300x106.jpg 300w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/concrete-powder-analysis.jpg 1418w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/p>\n<p><a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/particles-size-distr.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-large wp-image-977\" src=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/particles-size-distr-1024x718.jpg\" alt=\"particles size distr\" width=\"1024\" height=\"718\" srcset=\"https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/particles-size-distr-1024x718.jpg 1024w, https:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/particles-size-distr-300x210.jpg 300w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/a><\/p>\n<p>High quality nanoCT scans produce the best results, these take between 2-4 hrs per sample without any post processing. We can provide standard analysis such as particle size distribution analysis, within 1 hr after the scan. Analysis results (size distribution) can be e-mailed (CSV file) while volume data (10 Gb) is sent on hard drive with a free 3D viewer program. Academic rates are R550 per hour, excl 7% admin fee and VAT, commercial R1250 ph.<\/p>\n<p>Samples can be physically delivered to our labs (via courier) \u2013 for powders we need approx 2 x 2 x 2 mm for quantitative particle size distribution from 10-1000 micron<\/p>\n<p>This page is available as brochure: <a href=\"http:\/\/blogs.sun.ac.za\/ctscanner\/files\/2014\/10\/particle-analysis.pdf\">particle analysis<\/a><\/p>\n<p>Analysis performed in VGStudioMax 2.2<\/p>\n","protected":false},"excerpt":{"rendered":"<p>X-rays imaging at high resolution allows visualization and quantification of any type of sample, including particles and powders. X-ray computed tomography in the micro and even nano scale is now possible, as a service facility in Stellenbosch University. Here we present the advantages of using the method for particles and powder characterization. The full 3D &hellip; <\/p>\n<p><a class=\"more-link btn\" href=\"https:\/\/blogs.sun.ac.za\/ctscanner\/particle-size-distribution-analysis\/\">Continue reading<\/a><\/p>\n","protected":false},"author":9533,"featured_media":0,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[41662],"tags":[],"class_list":["post-972","post","type-post","status-publish","format-standard","hentry","category-powders-and-particles","item-wrap"],"_links":{"self":[{"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/posts\/972","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/users\/9533"}],"replies":[{"embeddable":true,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/comments?post=972"}],"version-history":[{"count":2,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/posts\/972\/revisions"}],"predecessor-version":[{"id":1905,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/posts\/972\/revisions\/1905"}],"wp:attachment":[{"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/media?parent=972"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/categories?post=972"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/blogs.sun.ac.za\/ctscanner\/wp-json\/wp\/v2\/tags?post=972"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}